摘要
为建立水产品中丙泊酚麻醉剂残留量的气相色谱测定方法,样品经乙酸乙酯提取, EMR-Lipid分散固相萃取管与EMR-polish反萃取管相结合净化, GC定量定性检测,内标法定量。结果表明:水产品中丙泊酚浓度在0.4~10.0μg/mL范围内其线性关系良好(R=0.999),加标回收率为83.75%~102.18%,相对标准偏差为1.54%~7.39%,检出限为0.3 mg/kg。该方法具有简便、省时、重现性好等特点,适用于水产品中丙泊酚的残留量的测定。
A gas chromatographic method for determining the residual amount of propofol anesthetic in aquatic products was established. The sample was extracted with ethyl acetate, and the purification of EMR-Lipid dispersed solid phase extraction tube combined with EMR-polish back extraction tube was qualitatively detected by GC and quantified by internal standard method. The results showed that the concentration of propofol in the range of 0.4-10.0 μg/mL was good(R=0.999), the recoveries were 83.75%-102.18%, and the relative standard deviation was 1.54%-7.39%. The detection limit was 0.3 mg/kg. The method had the characteristics of simplicity, time saving and good reproducibility, and it was suitable for determination of propofol residues in aquatic products.
作者
颜珲璘
黄和
高平
陈日檬
曾丹丹
周凯
YAN Huilin;HUANG He;GAO Ping;CHEN Rimeng;ZENG Dandan;ZHOU Kai(College of Food Science and Technology,Guangdong Ocean University,Zhanjiang 524088;Guangdong Provincial Key Laboratory of Aquatic Product Processing and Safety,Zhanjiang 524088;Key Laboratory of Advanced Processing of Aquatic Products of Guangdong Higher Education Institution,Zhanjiang 524088;Zhanjiang Institute for Food and Drug Control,Zhanjiang 524022)
出处
《食品工业》
CAS
北大核心
2020年第2期305-308,共4页
The Food Industry
基金
广东省科技计划项目(项目号:2014A02020812)
广东省湛江市非资助科技攻关计划项目(项目号:2018B01004).
关键词
水产品
丙泊酚
气相色谱
aquatic products
propofol
gas chromatographyl
