摘要
采用反相高效液相色谱 离子阱质谱法测定鸡肉中的氯霉素残留。鸡肉样品用乙腈进行提取 ,V(甲醇 )∶V( 0 .0 1mol L乙酸铵水溶液 ) =40∶60为流动相 ,采用ZorbaxEclipeseXDBC18柱进行分离 ,通过离子阱质谱 ,以选择离子反应进行检测。该方法的线性范围为 1～ 1 0 0 0 μg L ,样品的检出限为 0 .1 μg L。
A RP-HPLC-APCI-IT-MS method for the determination of chloramphenicol in chicken was described.The samples were extracted with acetonitrile,using methanol -ammonium acetate in water(40∶60 in volume ratio)as the mobile phase. The samples were separated with a zorbax eclipese XDB C18 column, and analysed by LC/MS with negative chemical ion detection. The detection limit was 0.1 μg/L.
出处
《分析试验室》
CAS
CSCD
北大核心
2004年第7期4-6,共3页
Chinese Journal of Analysis Laboratory
关键词
反相液相色谱
离子阱质谱
鸡肉
氯霉素
Reversed-phase liquid chromatography
Ion trap mass spectrometry
Chicken
Chlora mphenicol
