摘要
本文使用自制的负载有巯基碳粉的泡塑分离富集钯。试验了该富集剂对钯的最佳吸附与解脱条件以及23种共在离子的影响。对低钯管理样进行加标回收实验,结果表明,钯的平均回收率为89.65%,RSD=3.71%。
A new kind of foam plastic was made for theseparation and concentration of palladium. In themedium of 1% HCl,palladium can be adsorbed on themodified foam plastics completely by controlling theflow rate at 3mL/min. The adsorbed palladium can beduted with 2% NaBrO_3-2mol/L HCl as elutant,anddetermined by FAAS.23 coexisting ions have nointerference with the determination of palladium bythis method. The recoveries of palladium in samplesand the relative atandard deviation are satisfactory.
出处
《分析试验室》
CAS
CSCD
北大核心
1994年第6期28-29,共2页
Chinese Journal of Analysis Laboratory
关键词
泡塑分离富集
巯基碳粉
钯
Foam plastics
hydrosulfurylcarbonpowder
separation and concentration, palladiumdetermination