摘要
通过蒸发光散射检测器(ELSD)与高效液相色谱仪(HPLC)联用,可用反相C18色谱柱,以甲醇+0.1%三氟乙酸(TFA)水溶液=10+90(v+v)为流动相,分离检测草甘膦制剂中的草甘膦含量。草甘膦的相对标准偏差、平均回收率、线性范围分别为1.3%(n=9)、100.3%(n=5)、0.5￣2.5mg/ml(r=0.9994)。
An evaporative light scattering detector （ELSD） coupled with HPLC was used to separate and determine glyphosate content in a glyphosate formulation. The system used a reverse phase C18 column and a methanol ＋ 0.1% trifluoroacetic acid solution （10 ＋ 90% by vol） as the mobile phase. The relative standard deviation, average recovery,and range of concentration linearity were 1.3% （n=9）, 100.3% （n=5）, and 0.5 to 2.5 mg/ml （r=0.9994）, respectively.
出处
《农药》
CAS
北大核心
2005年第8期365-367,共3页
Agrochemicals
