摘要
由r─氯丙基三氯硅烧经醇解、胺取代、醇交换等反应制得1-(4,7,10-三氮杂癸基)-2,8,9-三氧杂-5-氮杂-1-硅杂[3.3.3.O1,5]十一烷.对该化合和光谱特征进行了表征,对质谱裂解机理进行了较详细地研究推导.
Triazadecyl )-2, 8, 9-trioxa-5-aza-1-silatricyclo[3. 3. 3. O1,5]undecane was synthesized from r-chloropropyltichloro silane by ethanolysis,aminosubstitution and alcohol exchange. Its spectra were studied.
出处
《山东大学学报(自然科学版)》
CSCD
1995年第2期236-242,共5页
Journal of Shandong University(Natural Science Edition)