摘要
采用微量液-液萃取法及气相色谱／质谱法对某种烟用香精的香味成分进行分离和鉴定，确认了其中的29种成分，并用峰面积归一化法测定了各种成分的百分含量，其主要成分为：柠檬烯（1．7255％）、薄荷醇（6．7434％）、丁子香酚（22．7645％）、反石竹烯（15．5365％）、α-啤酒花烯（1．8804％）、硬脂酸乙酯（41．8219％）等，相对标准偏差在3．44％～10．32％之间。结果证明，该方法是烟用香精质量控制中的一种快速、准确的分析方法。
Tobacco essence was isolated and identified by capillary GC/MS method. 29 Compounds were identified, the relative contents of constituents were determined by peak area normalization method. The main compositions were ： limonene （ 1. 7255% ）, menthol （ 6. 7434% ）, eugenol （ 22. 7645% ）, trans-caryophyllene （ 15. 5365% ）, α-humulene （ 1. 8804% ）, ethyl stearate （41.8219% ） etc. The relative standard deviations were between 3.44% and 10.32%. The results showed that this method was quick and accurate for quality control of tobacco essence.
出处
《应用化工》
CAS
CSCD
2006年第3期232-233,239,共3页
Applied Chemical Industry
