摘要
对中药中农药残留分析常用的前处理方法和检测分析方法进行了总结,并着重介绍了近年发展起来的一些农药残留前处理方法,如:固相微萃取、超临界流体提取、加速溶剂萃取、免疫亲和色谱等和残留检测分析的新技术,如:超临界流体色谱技术、柱切换高效液相技术、液相色谱-质谱联用技术、毛细管电泳和毛细管区带电泳技术、免疫分析技术等,这些将给中药中农药残留分析带来了很大的进步,并使中药中农药残留的分析逐步快捷、精确、标准。
The current methods to prepare and determine pesticide residues in Chinese herbal medicine were summarized in this paper. In addition, the new techniques to prepare and determine pesticide residues used in recent years was reviewed, which included solid-phase micro-extraction （SPME）, supercritical fluid extraction （SFE）, accelerated solvent extraction （ASE）, immune affinity chromatography （IAC）, supercritical fluid chromatography （SFC）, column switching high performance liquid chromatography （CSHPLC）, high performance liquid chromatography/mass spectrometrr （HPLC/MS）, capillary electrophoresis （CE） and capillary zone electrophoresis （CZE）, and immune analysis （IA） ,etc. To sum up, these would bring a great progress in analysis of the pesticide residues in Chinese herbal medicine, and make it more rapidly, accurately and normatively.
出处
《中国中药杂志》
CAS
CSCD
北大核心
2006年第22期1841-1846,共6页
China Journal of Chinese Materia Medica
基金
科技部科研院所社会公益研究专项(2004DIB1J039)
关键词
中药
农药残留
前处理
检测分析
Chinese herbal medicine
pesticide residues
preperation
determination and analysis
