摘要
Lu3Al5O12(LuAG) thin films with different Tb^3+ concentration were prepared on carefully cleaned (111 ) silicon wafer by a Peehini process and dip-coating technique. Heat treatment was performed in the temperature range from 800 to 1100 ℃. The crystal structure was analyzed by XRD. The results show that LuAG film starts to crystallize at about 900 ℃, and the particle size increases with the sintering temperature. Excitation and emission spectra of Tb^3+ doped LuAG films were measured. The effects of heat-treatment temperature and doping concentration of Th3 + on the luminescent properties were also investigated. For a comparison study, Th^3+-doped LuAG powders were also prepared by the same sol-gel method.
Lu3Al5O12(LuAG) thin films with different Tb^3+ concentration were prepared on carefully cleaned (111 ) silicon wafer by a Peehini process and dip-coating technique. Heat treatment was performed in the temperature range from 800 to 1100 ℃. The crystal structure was analyzed by XRD. The results show that LuAG film starts to crystallize at about 900 ℃, and the particle size increases with the sintering temperature. Excitation and emission spectra of Tb^3+ doped LuAG films were measured. The effects of heat-treatment temperature and doping concentration of Th3 + on the luminescent properties were also investigated. For a comparison study, Th^3+-doped LuAG powders were also prepared by the same sol-gel method.
基金
Project supported by the National High Technology Research and Development Programof China(863 Program) (2002 AA324070) and the National Natural Science Foundation of China (50332050)