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气相色谱/质谱法分析曼陀罗果实挥发油的化学成分 被引量:9

Analysis on Chemical Components of Volatile Oil in Fruit of Datura stramonium L. with GC/MS
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摘要 用水蒸汽蒸馏法从曼陀罗果实中提取挥发油,并用气相色谱/质谱(GC/MS)联用技术对其化学成分进行分离和结构鉴定,用峰面积归一化法确定各成分的相对含量。结果确定了68种化合物,占挥发油总量的82.83%,其主要成分为6-戊基-5,6-二氢化吡喃-2-酮(9.13%)、3,7,11,15-四甲基-2-十六碳烯-1-醇(6.71%)、二苯酮(6.16%)和1-己醇(6.10%)等。 The volatile oil was extracted from fruit of datura stramonium L. by water vapor distillation and the components of volatile oil were separated and structurally identified by gas chromatography/ mass spectrometry(GC/MS). The relative contents of the components were determined with the peakarea normalization method in gas chromatography. As a result, 68 compounds have been identified, accounting 82.83% of total volatile oil. The major components of the volatile oil were indentified as 6-pentyl-5, 6-dihydro-2 H-pyran-2-one ( 9. 13 % ), ( E)-3,7, 11,15-tetramethyl-2-hexadecen-1-ol ( 6. 71% ), benzophenone(6.16%) and 1-hexanol (6.10%).
出处 《分析科学学报》 CAS CSCD 2007年第6期697-700,共4页 Journal of Analytical Science
基金 陕西省教育厅科研计划项目(06JK305) 商洛学院科研资助项目(SKY05111)
关键词 曼陀罗 果实 挥发油 气相色谱/质谱 Datura stramonium L. Fruit Volatile oil GC/MS
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