摘要
本文对微波辐射下4,4’—二硝基二苯醚的两种合成方法进行了研究,结果表明,微波辐射可加快反应速度2~4倍,但不改变反应历程.
Two synthetic methods of 4, 4'-dinitrodiphenyl ether were studied under microwave ir-radiation. The results showed that the rate of the reaction was 2~4 fold in comparison withthat under conditions of classical heating,however the reaction mechanism remins the same.
关键词
二硝基二苯醚
微波辐射
有机合成
微波反应器
4, 4' -dinitrodiphenyl ether
microwave irradiation
organic synthesis