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PMBP缩磺胺席夫碱及其铜配合物的合成与抑菌活性 被引量：3

Synthesis and antibacterial activity of the Schiff base derived from PMBP and sulfanilamide and its transitional metallic copper complex
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摘要 In this paper,one novel Schiff base(HL) derived from 1-phenyl-3-methyl-4-benzoyl-pyrazolone-5(PMBP) and sulfanilamide and its corresponding transitional metallic copper complex have been synthesized in the nonaqueous solvent.The formula of complex is CuL2 based on elemental analysis,complexometric titration,molar conductance value and mass spectra data.Its molecular structure is characterized by means of IR,TG and 1HNMR,etc.,and the antibacterial activities under different concentrations of these two compounds are also measured with Oxford cup method. In this paper, one novel Schiff base （HL） derived from 1-phenyl-3-methyl-4-benzoyl- pyrazolone-5 （PMBP） and sulfanilamide and its corresponding transitional metallic copper complex have been synthesized in the nonaqueous solvent. The formula of complex is CuL2 based on elemental analysis ,complexometric titration ,molar conductance value and mass spectra data. Its molecular structure is characterized by means of IR, TG and ^1HNMR, etc. , and the antibacterial activities under different concentrations of these two compounds are also measured with Oxford cup method.
作者 李东颖 俞志刚 张桂玲
机构地区 哈尔滨理工大学化学与环境工程学院
出处 《化学研究与应用》 CAS CSCD 北大核心 2009年第3期406-409,共4页 Chemical Research and Application
基金 国家自然科学基金(50743013)资助项目 黑龙江省自然科学基金(E2007-35)资助项目 哈尔滨市青年科学基金(2005AFQXJ071)资助项目
关键词 席夫碱 铜配合物 合成 抑菌活性 Schiff base copper complex synthesis antibacterial activity
分类号 O614.33 [理学—无机化学] O626.21 [理学—有机化学]
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化学研究与应用
2009年 第3期

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