期刊文献+

吹扫捕集GC-MS法测定紫苏不同变种叶片中的挥发性成分 被引量:15

Purge and Trap GC-MS for the Identification of Volatile Composition of the Leaves of Different Variants of Perilla L.
在线阅读 下载PDF
导出
摘要 采用吹扫捕集技术对紫苏不同变种叶片中的挥发性成分进行富集,以气质联用仪(GC-MS)进行鉴定,运用面积归一化法确定各组分的相对含量。结果表明,分别属于紫苏属植物3个变种的4份试材之间叶片挥发油的组分和相对含量差异显著。4份紫苏试材共检测出31种挥发油成分,但其共有的成分仅有顺-3-己烯醛、石竹烯和圣亚麻三烯3种。野生紫苏变种的主要成分是柠檬烯(77.90%)、石竹烯(14.33%)、顺-3-己烯醛(4.9%)、胡椒酮(1.71%),回回苏变种的主要成分是石竹烯(30.65%)、柠檬烯(24.60%)、顺-3-己烯醛(21.82%)、紫苏醛(17.70%),紫苏变种1(来源于河北安国市)的主要成分是5-乙叉-1-甲基-环庚烯(52.79%)、顺-3-己烯醛(19.98%)、石竹烯(13.60%)、紫苏醛(9.46%),紫苏变种2(来源于广西灵山县)的主要成分是紫苏醛(31.86%)、5-乙叉-1-甲基-环庚烯(31.68%)、顺-3-己烯醛(21.50%)、石竹烯(10.47%)。 Purge and trap technique was used for enriching the volatile components of the leaves of different variants of Perilla L.prior to GC-MS analysis.Area normalization method was employed for the subsequent quantification.The results showed that there were significant differences in type and relative contents of volatile components among 4 samples belonging to 3 variants of Perilla L..Totally 31 volatile components were identified in the samples,3 of which,namely [Z]3-hexenal,caryophyllene and santolina triene were contained in all of the samples.The main components of the leaves of wild growing P.frutescens(Linn.) Britt.var.acuta(Thunb.) Kudo included limonene(77.90%),caryophyllene(14.33%),[Z]-3-hexenal(4.9%),and 3-methyl-6-[1-methethyl]-2-cyclohexen-1-one(1.71%),those of the leaves of P.frutescens(Linn.) Britt.var.crispa(Benth.)H.W.Li caryophyllene(30.65%),limonene(24.60%),[Z]-3-hexenal(21.82%) and perilla aldehyde(17.70%),and those of the sample No.1 of P.frutescens(Linn.)Britt.var.frutescen from Anguo,Hebei province 5-ethylidene-1-methyl-cycloheptene(52.79%),[Z]-3-hexenal(19.98%),caryophyllene(13.60%) and perilla aldehyde(9.46%),and those of the sample No.2 of P.frutescens(Linn.)Britt.var.frutescen from Linshan,Guangxi autonomous region perilla aldehyde(31.86%),5-ethylidene-1-methyl-cycloheptene(31.68%),[Z]-3-hexenal(21.50%) and caryophyllene(10.47%).
出处 《食品科学》 EI CAS CSCD 北大核心 2010年第12期159-164,共6页 Food Science
基金 河北省科技攻关项目(07276410D) "十一五"国家科技支撑计划重大专项(2009ZX09308-002)
关键词 吹扫捕集技术 气相色谱-质谱法(GC-MS) 紫苏属 挥发性成分 相对含量 purge and trap technique GC-MS Perilla L. volatile substances relative content
  • 相关文献

参考文献45

  • 1NITTA M, LEE J K, OHNISHI O. Asian Perilla crops and their weedy forms: their cultivation, utilization and genetic elationships[J]. Society for Economic Botany, 2003, 57(2): 245-253.
  • 2国家药典委员会.中华人民共和国药典:一部[M].北京:人民卫生出版社.1990:39.
  • 3田妹华.出口日本青紫苏优质高效栽培技术[J].长江蔬菜,2008(4):20-22. 被引量:5
  • 4殷朝洲.紫苏的开发利用[J].上海农业科技,1989(2):17-19. 被引量:5
  • 5本多义昭,沙振方.从紫苏中分离延长小鼠睡眠的时萝芹菜脑[J].国外医药(植物药分册),1989,4(3):125-126. 被引量:9
  • 6KERR L A, JOHNSON B J. Intoxication of cattle by Perillafrutescens (purplemint)[J]. Vet Hum Toxic, 1986, 28: 412-416.
  • 7ABERNATHY V J, ROSELLI R J. Effects of Perilla ketone on the in situ sheep lung[J]. J Appl Physiol, 1992, 72(2): 505-514.
  • 8WILSON B J, GARST J E, CHANNEL R B. Perilla ketone: a potent lung toxin from the mint plant, Perillafrutescens Britt[J]. Science, 1977, 197: 573-574.
  • 9KANG R, HELMS R, STOUT M J, et al. Antimicrobial activity of the volatile constituents of Perillafrutescens and its synergistic effects with polygodial[J]. J Agric Food Chem, 1992, 40(11): 2328-2330.
  • 10THONGDON A J, INPRAKHON P. Composition and biological activities of essential oils from Limnophila geoffrayi Bonati[J]. World Journal of Microbiology and Biotcchnology, 2009, 25(8): 1313-1320.

二级参考文献48

共引文献192

同被引文献225

引证文献15

二级引证文献133

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部