摘要
目的:对毛茛科铁线莲属植物山木通的化学成分进行提取、分离和鉴定。方法:用不同浓度乙醇提取,利用硅胶、Sephadex LH-20、ODS柱色谱法对山木通的化学成分进行分离,根据理化性质和MS、NMR光谱数据进行结构鉴定。结果:经鉴定得到7个化合物,分别为β-谷甾醇(I);正二十二烷(II);3-羰基齐墩果烷(III);正十六烷酸(IV);正二十六烷酸(V);丁香酸(VI);5-羟基4-氧代戊酸(VII)。结论:所得化合物均为首次从该种植物中得到。
Objective： To study the chemical constituents from Clematisfinetiana L6vl. et Vant. Method： The chemical constituents were extracted by alcohol of different concentrations and isolated by silica gel, Sephadex LH -20, ODS column chromatographic method. The chemical structures of components were further elucidated by the physicochemical characters and MS, NMR spectral data. Results： Seven chemical constituents were isolated and identified from Clematis flnetiana Levi. et Vant. They were β- sitosterol （Ⅰ）, docosane （Ⅱ）, 3 - ketooleanane （Ⅲ）, n - hexadecanoic acid （Ⅳ）, hexacosanoic acid （Ⅴ） ; eugenol （Ⅵ） ; 5 -hydroxy-4 -oxopentanoic acid（Ⅶ）. Conclusion： All the compounds were isolated from the plant for the first time.
出处
《中国野生植物资源》
2011年第2期39-41,共3页
Chinese Wild Plant Resources
基金
国家自然科学基金(30772770)
关键词
山木通
化学成分
3-羰基齐墩果烷
正十六烷酸
正二十六烷酸
丁香酸
5-羟基4-氧代戊酸
Clematis finetiana Levi. et Vant.
chemical constituents
3 - ketooleanane
n - hexadecanoic acid
hexacosanoic acid
eugenol
5 - hydroxy - 4 - oxopentanoic acid
