摘要
采用微波消解,ICP-MS法测定国内10种调味料中有毒和必须金属元素含量,测定标准物质对方法进行确证。结果表明,方法的相对标准偏差小于5%,回收率在83.4%~115%之间。调料中K、Ca、Mg、Mn、Fe含量丰富,生姜中As含量较高,桂皮和花椒中Pb含量高。
Toxic and essential metal element content of ten different spices of China were determined by ICP-MS after microwave digestion method.The validation of the presented procedure is performed by the analysis of standard reference material.The relative standard deviations were found to be lower than 5%,and the recovery values were 83.4%～115%.The contents of K,Ca,Mg,Mn,Fe are rich in all the spices,the content of As is high in ginger and the content of Pb is high in cassia and prickly ash.
出处
《中国调味品》
CAS
北大核心
2011年第8期95-97,105,共4页
China Condiment
