Amide Hydrolysis Reaction Catalyzed by KF/Al2O3 under Microwave Irradiation and Solvent Free Conditions
Amide Hydrolysis Reaction Catalyzed by KF/Al2O3 under Microwave Irradiation and Solvent Free Conditions
摘要
A microwave-enhanced hydrolysis of amides utilizing KF/Al2O3 in the absence of solvents has been developed. Amines are produced in excellent yields along with the corresponding carboxylic acids.
A microwave-enhanced hydrolysis of amides utilizing KF/Al2O3 in the absence of solvents has been developed. Amines are produced in excellent yields along with the corresponding carboxylic acids.
基金
Project supported by the National Natural Science Foundation of China （No. 0972057）.
参考文献33
-
1Greene, T. W.; Wuts, P. G. M. Protective Groups in Organic Synthesis, 3rd ed., John Wiley and Sons, New York, 1999.
-
2Gassman, P. G.; Hodgson, P. K. G.; Balchunis, R. J. J. Am. Chem. Soc. 1976, 98, 1275.
-
3Singh, L.; Ram, R. N. J. Ore. Chem. 1994, 59, 710.
-
4Evans, D. A.; Carter, P. H.; Dinsmore, C. J.; Barrow, J. C.; Katz, J. L.; Kung, D. W. Tetrahedron Lett. 1997, 38, 4535.
-
5Karanewsky, D. S.; Malley, M. F.; Gougoutas, J. Z. J. Org. Chem. 1991, 56, 3744.
-
6Kabalka, G. W.; Wang, L.; Pagni, R. M. Synlett 2001, 261.
-
7Kabalka, G. W.; Pagni, R. M. Tetrahedron 1997, 53, 7999.
-
8McGinnis, M. B,; Vagle, K.; Green, J. F.; Tan, L. C.; Palmer, R.; Siler, J.; Pagni, R. M.; Kabalka, G. W. J. Org. Chem. 1996, 61, 3496.
-
9Wilgus, C. P.; Downing, S.; Molitor, E.; Bains, S.; Pagni, R. M.; Kabalka, G. W. Tetrahedron Lett. 1995, 36, 3469.
-
10Sponholtz III, W. R.; Pagni, R. M.; Kabalka, G. W.; Green, J. F.; Tan, L. C. J. Org. Chem. 1991, 56, 5700.
-
1林棋,吕吓强,何明顺,陈书勤.微波辐射KF/Al_2O_3催化合成肉桂醛[J].闽江学院学报,2001,22(2):59-61. 被引量：5
-
2许皓诚,冯乙巳,汪鹏飞.固体碱KF/Al_2O_3合成烯丙基缩水甘油醚[J].安徽化工,2014,40(4):20-22. 被引量：1
-
3张玮,雷阿旺,赵志利.固体碱催化合成假性紫罗兰酮研究[J].广州化工,2010,38(5):157-158. 被引量：7
-
4沈润溥,孔识卫,胡四平,陈春峰,张伯引,王再中.KF/Al_2O_3催化反应精馏制备1-羟基-2-甲基-4-乙酰氧基-2-丁烯的研究[J].江苏化工,2006,25(17):16-18.
-
5荣良策,韩红霞,蒋虹,庄启亚,王香善,屠树江.KF-Al_2O_(3)催化下2-氨基-6-甲基-4-芳基-1,3-二氰基苯衍生物的合成[J].有机化学,2008,28(8):1454-1456.
-
6王洪波,马敬中,陈冬玲.用KF/Al_2O_3催化合成肉桂酸的研究[J].内蒙古石油化工,2002,28(4):9-10.
-
7张家仁,白荣献,李光兴.KF/Al_2O_3催化菜籽油与甲醇合成生物柴油的研究[J].现代化工,2006,26(11):45-46. 被引量：20
-
8KF／Al2O3催化合成肉桂醛[J].精细化工经济与技术信息,2001(5):17-17.
-
9王洪波,马敬中,陈冬玲.用KF/Al_2O_3催化合成肉桂酸的研究[J].湖北化工,2002,19(6):26-27. 被引量：3
-
10杨秀英,彭安顺.KF/Al_2O_3催化合成苄叉丙酮[J].临沂师范学院学报,2001,23(4):48-49. 被引量：3
