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地锦草挥发性成分的HS-SPME-GC-MS分析 被引量:9

Volatile Compounds from Euphorbia humifusa
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摘要 目的:研究地锦草的挥发性成分。方法:采用顶空固相微萃取-气质联用技术对地锦草全草挥发性成分进行分析和鉴定,并用峰面积归一化法计算其相对百分含量。结果:从地锦草中共鉴定出22种成分,相对含量占挥发性成分总峰面积的93.89%,其中主要成分为酮(32.33%)、酸(25.32%)和酯(14.55%)等。结论:研究表明含量较高的挥发性成分为棕榈酸(20.35%)、植醇(16.41%)和2-甲氧基-4-乙烯苯酚(10.98%)。其中二氢猕猴桃内酯和可巴烯可能是地锦草主要的赋香成分。 Objective: To study the volatiles from E. humifusa Method: The volatile compounds from Euphorbia humifusa were extracted by head-space solid-phase micro-extraction (HS-SPME) coupled with gas chromatography-mass spectrometry (GC-MS). A quantitative analysis in percentage was performed by peak area normalization measurements. Result: Twenty-two compounds were identified, presenting for 93.89% of total volatiles. The volatile constituents were mainly ketones (32.33%), acids (25.32%) , esters ( 14.55% ) , and other substances. Conclusion: The main compounds were N-hexadecanoic acid (20.35%), phytol ( 16.41% ), 2-methoxy-4-vinylphenol (10.98%) and so on. The main fragrance constituents were dihydroactindiolide and copaene.
出处 《中国实验方剂学杂志》 CAS 北大核心 2012年第21期66-68,共3页 Chinese Journal of Experimental Traditional Medical Formulae
基金 河南省科技厅重点攻关项目(102102310019)
关键词 地锦草 挥发性成分 固相微萃取 气相色谱-质谱法 Euphorbia humifusa volatile compounds SPME GC-MS
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