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5-硝基水杨酸合成工艺的改进 被引量:11

AN IMPROVED TECHNIQUE FOR THE SYNTHESIS OF 5-NITRO-SALICYLIC ACID
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摘要 用负载型稀土催化剂 ,在无水乙醇介质中 ,用浓硝酸硝化水杨酸 ,使 5 -硝基水杨酸的产率提高到了 80 %以上 ,同时考察了反应温度、反应时间对产率的影响 。 The nitrification of salicylic acid with nitric acid was studied by using supported rare earth as catalysts and ethanol as solvent.The yield of 5\|nitro\|salicylic acid was raised up to 80%.The influences of temperature and reaction time on the yield of the product were investigated,and the optinum condition was acquired.
出处 《甘肃科学学报》 2000年第3期54-55,共2页 Journal of Gansu Sciences
基金 甘肃省自然科学基金资助项目!( ZR97-0 0 5)
关键词 硝化 5-硝基水杨酸 负载型稀土催化剂 合成工艺 salicylic acid nitrification rare earth
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  • 1贾建洪,盛卫坚,陈斌,高建荣.5-硝基水杨酸的合成新工艺研究[J].浙江工业大学学报,2005,33(1):96-99. 被引量:3
  • 2陆涛,尤启冬.马沙拉嗪合成工艺改进[J].现代应用药学,1994,11(1):32-32. 被引量:5
  • 3郑家驹.氨基水杨酸盐治疗炎症性肠病的药理学研究[J].中国药房,2005,16(13):1025-1028. 被引量:15
  • 4朱锦江 韩翠琳 等.马沙拉嗪的合成[J].中国医药工业杂志,1991,22(7):295-295,301.
  • 5Liao Xiangjtm, Raghavana G S V, Yaylayan V A. A novel way to prepare n - butylparaben under microwave irradiation[J]. Tetrahedron Letters, 2002, 43:45 -48
  • 6Gedye R, Smith F, Westaway K. , et al. The use of microwave for rapid organic synthesis [ J ]. Tetrahedron Letters, 1986, 27 : 279 - 282
  • 7Sadfler resereh laboratories division of Bio - rad laboratories Standard infrared grating spectra [ M ]. INC Reserehers, Editors, Publishers, Printed USA, 1980, 9 - 10: 8424
  • 8Almog J, Klein A, Sokol A, et al. Urea nitrate and nitrourea: powerful and regioselective aromatic nitration agents[J]. TetrahedronLetters, 2006, 47(49): 8 651.
  • 9Fox JJ, Su TL, Stempel LM, et al. Pyrimidines. 18. A novel pyrirnidine to benzene ring transformation reaction. Conversion of 5-nitro-2 ( 1 H)-pyrimidinone into p-nitrophenol derivatives[J]. J Org Chem, 1982,47 ( 6 ) : 1 081.
  • 10韩广甸 赵树纬 等.有机制备化学手册(上卷)[M].北京:石油化学工业出版社,1978.153-171.

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