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基于无机元素分析的当归烟熏加工工艺优选 被引量:5

Optimization of Smoked Processing Technology of Angelicae Sinensis Radix Based on Analysis of Inorganic Elements
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摘要 目的:探讨不同烟熏条件加工的当归药材中15种无机元素的含量及分布特征,确定最佳烟熏加工工艺。方法:采用ICP-MS测定31个烟熏当归样品中8种重金属元素含量,AAS测定其他7种无机元素含量,利用IBM SPSS 21.0及SIMCA-P 11.5软件进行统计分析。结果:不同烟熏条件加工的当归药材中无机元素特征性指纹表现为K>Na>Cr>Cu的趋势;烟熏温度是影响烟熏当归药材中无机元素分布的最关键因素;最佳烟熏加工工艺为50℃烟熏8 h。结论:调控温度和时间进行烟熏加工的当归药材安全性良好。 Objective: To investigate contents and distribution characteristics of 15 kinds of inorganic elements in Angelicae Sinensis Radix smoked by different processing conditions, and to determine optimum smoked processing technology. Method: Contents of 8 heavy metal elements in 31 smoked samples were determined by ICP-MS, and the other 7 inorganic elements were determined by AAS, IBM SPSS 21.0 and SIMCA-P 11.5 statistical software were used for statistical analysis. Result: Fingerprint characteristic of inorganic elements in Angelicae Sinensis Radix smoked by different processing conditions showed the same trend of K 〉 Na 〉 Cr 〉 Cu;. temperature was the key factor affecting distribution of inorganic elements in smoked Angelicae Sinensis Radix; optimal smoked processing conditions were smoked for 8 hours at 50 ℃. Conclusion: Smoked processing of Angelicae Sinensis Radix had good safety by regulation of temperature and time.
出处 《中国实验方剂学杂志》 CAS 北大核心 2014年第11期1-6,共6页 Chinese Journal of Experimental Traditional Medical Formulae
基金 国家自然科学基金项目(30960037) 甘肃省发改委战略新兴产业和产业技术研究与开发专项[2011]
关键词 当归 烟熏 无机元素指纹图谱 电感耦合等离子体质谱法 原子吸收光谱法 聚类分析 Angelicae Sinensis Radix smoked processing fingerprint of inorganic elements ICP-MS AAS cluster analysis
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