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夏季红茶摇青发酵工艺优化及香气成分的SPME-GC/MS分析 被引量:10

Study on the Shaking-fermentation Process Optimization and SPME-GC/MS Analysis of Aromatic Components of Summer Black Tea
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摘要 开展摇青发酵工艺在夏季红茶加工中的应用研究,分析其香气组分,为提高夏季红茶品质提供理论基础。采取L9(34)正交试验方法,优化夏季红茶摇青发酵工艺。采取固相微萃取和气相色谱-质谱(SPME-GC/MS)对摇青发酵红茶香气成分进行分析。夏季摇青发酵红茶优化工艺参数为:萎凋时间14 h、摇青时间55 min、堆积发酵时间4.0 h,在该工艺参数下制作的红茶具有明显甜花香。在摇青发酵红茶中共检测出83种香气成分,包括醇类、酯类、醛类、烯烃类和酮类等,其中醇类和酯类化合物含量较高,以苯乙醇、芳樟醇及其氧化物、香叶醇、3,7-二甲基-1,5,7-辛三烯-3-醇、水杨酸甲酯等17种化合物为主体,占香气成分总量的61.34%,是形成摇青发酵红茶甜花香的重要组分,而3,7-二甲基-1,5,7-辛三烯-3-醇可能是形成摇青发酵红茶甜花香的特殊成分。同时检出了β-环柠檬醛、柠檬醛等31种对照中未检出的香气成分。摇青发酵可增加红茶香气组分,有利于提高夏季红茶香气品质。 Study on the shaking-fermentation process of the summer black tea, analyze the aroma components of black tea prepared with the method of shaking-fermentation, and provide a theoretical basis to improve the quality of summer black tea. The optimization of shaking-fermentation process of summer black tea was optimized by L9(3^4) orthogonal test method, and the aroma components of black tea prepared with shaking-fermentation method were detected by SPME-GC/ MS. The optimization of process parameters of shaking-fermentation was as follows: Withering time was 14 h, shaking time was 55 min and fermentation time was 4.0 h. Under the process parameters, there existed obvious sweet floral in the black tea. A total of 83 aromatic components were detected in the summer black tea prepared with shaking-fermentation process, which included alcohols, esters, aldehydes, olefins and ketones, and the content of alcohols and esters was higher. A total of 17 components were the main aromatic component, which included benzene ethanol, linalool and its oxides, geraniol, 3, 7-dimethyl-1, 5, 7-octatrien-3-ol, salicylic acid and so on, their total content reached to 61.34%, they could be the important components that form the sweet floral, and the component of 3, 7-dimethyl-1, 5, 7-octalrien-3-ol was the special aroma for sweet floral, probably. Meanwhile, a total of 31 aromatic components including beta-cyclocitral, (E)-citral and others were detected meanwhile they weren't detected in the rolling-fermentation black tea. Shaking-fermentation could increase the aroma components of black tea, which was beneficial to improve the aroma quality of the summer black tea.
出处 《食品工业》 CAS 北大核心 2017年第3期164-168,共5页 The Food Industry
基金 四川省教育厅科技项目基金(15ZB-0496) 宜宾市自然科技基金(2014NY-019)
关键词 夏季红茶 摇青发酵 正交试验 香气成分 GC/MS分析 summer black tea shaking-fermentation orthogonal test aromatic component GC/MS analysis
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