摘要
采用水热还原法制备了不同还原程度的还原氧化石墨烯(RGO),并将其添加到水泥浆体中,制得石墨烯增强水泥基复合材料。采用傅里叶变换红外光谱(FT-IR)、力学性能测试仪、扫描电子显微镜(SEM)对氧化石墨烯(GO)还原程度及水泥基复合材料的力学性能和微观结构进行测试。结果表明,在120℃水热条件下,控制不同还原时间可以得到不同还原程度的RGO;随着GO还原程度的提高,复合材料力学强度不断增加;RGO可使水泥更加密实,降低了水泥浆体的孔隙率,对水泥基复合材料起到增强增韧的作用。
Reduced graphene oxide(RGO) with different degrees of reduction has been prepared by the hydrothermal reduction method and then was added to cement slurry to obtain grapheme-reinforced cement-based composites. Subsequently, the reduction degree of graphene oxide(GO), mechanical properties and microstructure of cement-based composites were characterized by Fourier Transform infrared spectroscopy(FT-IR), mechanical property tester and scanning electron microscopy(SEM). The results show that under the hydrothermal temperature of 120℃, RGO with different reduction degrees can be obtained by controlling the reduction time;with the increase of GO reduction degrees, the mechanical strength of composites increases constantly;RGO can make the cement more compact,which reduces the porosity of the cement slurry and plays an important role in strengthening and toughening the cement-based composite materials.
作者
刘洪丽
曹家豪
李亚静
潘华
韩雪
李婧
Liu Hongli;Cao Jiahao;Li Yajing;Pan Hua;Han Xue;Li Hongyan;Li Jing(State Key Laboratory of Green Building Materials,Beijing 100024,China)
出处
《水泥工程》
CAS
2020年第1期7-10,共4页
Cement Engineering
关键词
氧化石墨烯
水泥基复合材料
还原程度
力学性能
微观结构
Graphene oxide
Cement-based composites
Reduction degree
Mechanical properties
Microstructure
