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Incorporating empirical knowledge into data-driven variable selection for quantitative analysis of coal ash content by laser-induced breakdown spectroscopy 被引量:1
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作者 吕一涵 宋惟然 +1 位作者 侯宗余 王哲 《Plasma Science and Technology》 SCIE EI CAS CSCD 2024年第7期148-156,共9页
Laser-induced breakdown spectroscopy(LIBS)has become a widely used atomic spectroscopic technique for rapid coal analysis.However,the vast amount of spectral information in LIBS contains signal uncertainty,which can a... Laser-induced breakdown spectroscopy(LIBS)has become a widely used atomic spectroscopic technique for rapid coal analysis.However,the vast amount of spectral information in LIBS contains signal uncertainty,which can affect its quantification performance.In this work,we propose a hybrid variable selection method to improve the performance of LIBS quantification.Important variables are first identified using Pearson's correlation coefficient,mutual information,least absolute shrinkage and selection operator(LASSO)and random forest,and then filtered and combined with empirical variables related to fingerprint elements of coal ash content.Subsequently,these variables are fed into a partial least squares regression(PLSR).Additionally,in some models,certain variables unrelated to ash content are removed manually to study the impact of variable deselection on model performance.The proposed hybrid strategy was tested on three LIBS datasets for quantitative analysis of coal ash content and compared with the corresponding data-driven baseline method.It is significantly better than the variable selection only method based on empirical knowledge and in most cases outperforms the baseline method.The results showed that on all three datasets the hybrid strategy for variable selection combining empirical knowledge and data-driven algorithms achieved the lowest root mean square error of prediction(RMSEP)values of 1.605,3.478 and 1.647,respectively,which were significantly lower than those obtained from multiple linear regression using only 12 empirical variables,which are 1.959,3.718 and 2.181,respectively.The LASSO-PLSR model with empirical support and 20 selected variables exhibited a significantly improved performance after variable deselection,with RMSEP values dropping from 1.635,3.962 and 1.647 to 1.483,3.086 and 1.567,respectively.Such results demonstrate that using empirical knowledge as a support for datadriven variable selection can be a viable approach to improve the accuracy and reliability of LIBS quantification. 展开更多
关键词 laser-induced breakdown spectroscopy(LIBS) coal ash content quantitative analysis variable selection empirical knowledge partial least squares regression(PLSR)
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Calorific values and ash contents of different parts of Masson pine trees in southern China 被引量:4
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作者 Wei-sheng ZENG Shou-zheng TANG Qian-hui XIAO 《Journal of Forestry Research》 SCIE CAS CSCD 2014年第4期779-786,共8页
Calorific value of plants is an important parameter for evalu- ating and indexing material cycles and energy conversion in forest eco- systems. Based on mensuration data of 150 sample sets, we analyzed the calorific v... Calorific value of plants is an important parameter for evalu- ating and indexing material cycles and energy conversion in forest eco- systems. Based on mensuration data of 150 sample sets, we analyzed the calorific value (CV) and ash content (AC) of different parts of Masson pine (Pinus massoniana) trees in southern China using hypothesis testing and regression analysis. CV and AC of different tree parts were almost significantly different (P〈0.05). In descending order, ash-free calorific value (AFCV) ranked as foliage 〉 branch 〉 stem bark 〉 root 〉 stem wood, and AC ranked as foliage 〉 stem bark 〉 root 〉 branch 〉 stem wood. CV and AC of stem wood from the top, middle and lower sections of trees differed significantly. CV increased from the top to the lower sections of the tnmk while AC decreased. Mean gross calorific value (GCV) and AFCV of aboveground parts were significantly higher than those of belowground parts (roots). The mean GCV, AFCV and AC of a whole tree of Masson pine were 21.54 kJ/g, 21.74 kJ/g and 0.90%, re- spectively. CV and AC of different tree parts were, to some extent, cor- related with tree diameter, height and origin. 展开更多
关键词 ash-free calorific value ash content gross calorific value hypothesis testing regression analysis Pinus massoniana
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Preparation of activated carbon with low ash content and high specific surface area from coal in the presence of KOH 被引量:1
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作者 解强 陈清如 +2 位作者 宫国卓 张香兰 许德平 《Journal of Coal Science & Engineering(China)》 2003年第2期84-89,共6页
An activated carbon with ash content less than 10% and specific surface area more than 1 600 m 2 /g was prepared from coal and the effect of K containing compounds in preparation of coal based activated carbon was inv... An activated carbon with ash content less than 10% and specific surface area more than 1 600 m 2 /g was prepared from coal and the effect of K containing compounds in preparation of coal based activated carbon was investigated in detail in this paper. KOH was used in co carbonization with coal, changes in graphitic crystallites in chars derived from carbonization of coal with and without KOH were analyzed by X ray diffraction (XRD) technique, activation rates of chars with different contents of K containing compounds were deduced, and resulting activated carbons were characterized by nitrogen adsorption isotherms at 77 K and iodine numbers. The results showed that the addition of KOH to the coal before carbonization can realize the intensive removal of inorganic matters from chars under mild conditions, especially the efficient removal of dispersive quartz, an extremely difficult separated mineral component in other processes else. Apart from this, KOH demonstrates a favorable effect in control over coal carbonization with the goal to form nongraphitizable isotropic carbon precursor, which is a necessary prerequisite for the formation and development of micro pores. However, the K containing compounds such as K 2 CO 3 and K 2 O remaining in chars after carbonization catalyze the reaction between carbon and steam in activation, which leads to the formation of macro pores. In the end an innovative method, in which KOH is added to coal before carbonization and K containing compounds are removed by acid washing after carbonization, was proposed for the synthesis of quality coal based activated carbon. 展开更多
关键词 coal based activated carbon KOH ash content specific surface area
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Prediction of ash content of unloaded coal based on a discrete element simulation
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作者 Deng Jianjun Zhuo Jinwu Shi Hongxia 《International Journal of Mining Science and Technology》 SCIE EI 2013年第5期647-651,共5页
Based on analysis of regularity of stacking coal,discrete element simultaneous simulation is adopted to predict the process of unloading coal,which is proved to be effcient in the prediction of ash content.The results... Based on analysis of regularity of stacking coal,discrete element simultaneous simulation is adopted to predict the process of unloading coal,which is proved to be effcient in the prediction of ash content.The results show that the altitude of new irregular coal is equal to the income coal volume divided by area of cabin.The distribution of infnitesimal flow velocity helps to induce the motion equation of infnitesimal element,which provides the mathematical model for computer simulation.Swarm,a computer programming language,is utilized in this study.Adaptive infnitesimal stacking algorithm helps settle the diffculties in attainment of infnitesimal elements.The result of simulation is similar to the actual situation,which can accurately predict the ash contents of current time and cumulative time.Coal movement in the cabin is a new project,the result of which can also be applied to other solid particles and the widespread of the result will be highly valued. 展开更多
关键词 Discrete element SIMULATION ash content forecast Coal blending Motion equation Mathematical model
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Determination of Ash Contents in Coal by Means of Ordinary Kriging Method
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作者 Tomasz Niedoba Tadeusz Tumidajski 《Journal of Earth Science and Engineering》 2012年第10期571-575,共5页
The ash contents in coal particles were examined in the paper dependably on particle size and its density. So, the two-dimensional regressive function Z = Z(P, D) was the searched object, where Z is random variable ... The ash contents in coal particles were examined in the paper dependably on particle size and its density. So, the two-dimensional regressive function Z = Z(P, D) was the searched object, where Z is random variable describing ash contents, P---density and D---particle diameter. This dependence was determined based on experimental data concerning the coal of type 31. For this coal, the method of ordinary kriging was applied to calculate the values of random variable Z. This method required the proper selection of so-called variogram function, in which four forms were considered in this paper in purpose to select the best solution. The given results were then evaluated by the mean standard error value and compared with empirical data. 展开更多
关键词 Ordinary kriging COAL ash contents geostatistics.
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FAST MEASUREMENT OF ASH CONTENT IN COAL WASHING PLANT
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作者 马永和 罗向东 杨大战 《Nuclear Science and Techniques》 SCIE CAS CSCD 1993年第2期95-100,共6页
The coal filter cake is a product of fine coal after floatation which has an ash content of 7-13%, water content of 30±2%, and a particle size of less than 1 mm. The ash content was measured by the intensity of t... The coal filter cake is a product of fine coal after floatation which has an ash content of 7-13%, water content of 30±2%, and a particle size of less than 1 mm. The ash content was measured by the intensity of the single backscattered gamma-ray, and its accuracy is mainly dependent on the energy of the gamma-ray. The 238Pu low energy photon source is selected in this work. The energy of its gamma-ray is 15 keV, which can result not only in the best sensitivity, but also in the lowest contribution to the environment radiation. The root mean square deviation of the ash measurement is±0.33% (±1σ). 展开更多
关键词 COAL filter CAKE GAMMA RAY BACKSCATTERING ash content
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Quality Evaluation of Yi Medicine "Qibujing" Based on Determination of Water Content and Ash Content
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作者 Xuexue LI Hongna SU +5 位作者 Ying LI Xiaoxia CAI Risha WEIZE Zhengming YANG Yingfen HAO Yuan LIU 《Medicinal Plant》 CAS 2020年第1期67-68,92,共3页
[Objectives]To determine the water content,total ash content and acid-insoluble ash content of Yi medicinal material"Qibujing",so as to provide experimental basis for establishing the Quality Standard(Draft)... [Objectives]To determine the water content,total ash content and acid-insoluble ash content of Yi medicinal material"Qibujing",so as to provide experimental basis for establishing the Quality Standard(Draft)of Yi Medicinal Material"Qibujing"in Sichuan Province.[Methods]According to the second method(drying method)in 0832 water content determination method and 2301 ash content determination method in Chinese Pharmacopoeia(2015 Edition),it was determined,respectively,and the data were processed by IBM SPSS Statistics 26 and DPS 7.05 data processing system.[Results]All the 14 batches of sample met the stipulation that the water content should not exceed 12.0%,the total ash content should not exceed 8.0%,and the acid-insoluble ash content should not exceed 1.5%under"Guan Zhong-(Qibujing)"in the 2005 edition of Yunnan Traditional Chinese Medicine Standard.There was a negative correlation between water content,acid-insoluble ash content and altitude,and a positive correlation between total ash content and altitude.[Conclusions]It is suggested that Quality Standard(Draft)of Yi Medicinal Material"Qibujing"in Sichuan Province stipulate that the water content should not exceed 12.0%,the total ash content should not exceed 8.0%,and the acid-insoluble ash content should not exceed 1.5%. 展开更多
关键词 YI medicine"Qibujing" POTENTILLA fulgens WATER content ash content content DETERMINATION
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Determination of Moisture, Ash, Extract Content and TLC identification of Tibetan Medicinal Material Dracocephalum tanguticum Maxim. 被引量:1
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作者 Pei QUN Risha WEIZE +3 位作者 Zhe LIU Haiyan XIANG Yunzhang XU Yuan LIU 《Medicinal Plant》 CAS 2019年第4期51-53,59,共4页
[Objectives] The moisture, ash and extract content of Dracocephalum tanguticum Maxim. were measured.[Methods] The moisture, total ash, acid-insoluble ash and extract content of D. tanguticum Maxim collected from 16 pr... [Objectives] The moisture, ash and extract content of Dracocephalum tanguticum Maxim. were measured.[Methods] The moisture, total ash, acid-insoluble ash and extract content of D. tanguticum Maxim collected from 16 producing areas were detected by using the methods in Chinese Pharmacopoeia (2015 edition, volume I), and D. tanguticum Maxim. was identified by thin layer chromatography in Chinese Pharmacopoeia (2015 edition, volume I).[Results] The moisture content of D. tanguticum Maxim collected from 16 producing areas ranged from 8.68% to 10.36%, averaging 9.28%. The content of total ash was between 7.21% and 11.60%, averaging 9.89%. The content of acid-insoluble ash was 0.21%-2.71%, averaging 1.51%. The extract content (water-soluble) was 26.67%-42.91%, averaging 32.65%. According to the results of TLC identification, the 16 samples and reference substance had the same characteristic spots at the corresponding positions.[Conclusions] It was recommended that the moisture, total ash and acid-insolue ash content of D. tanguticum Maxim were not be more than 11%, 12%, and 3% respectively, while the extract content was not less than 26%. It provides reference for filling the gaps in the quality standards of D. tanguticum Maxim. 展开更多
关键词 TIBETAN MEDICINAL MATERIAL Dracocephalum tanguticum MAXIM MOISTURE ash Extract content TLC
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Evaluation of Wild Paeonia veitchii Lynch from Sichuan Based on Moisture, Ash and Extract Contents
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作者 Fang XIAO Xuexue LI +3 位作者 Jixiu SHEN Xiaoxia CAI Zhengming YANG Yuan LIU 《Medicinal Plant》 CAS 2020年第1期76-79,共4页
[Objectives]The research aimed to determine the contents of moisture,ash and extract of wild Paeonia veitchii Lynch produced in Sichuan,so as to provide the basis for evaluating quality of wild P.veitchii Lynch from S... [Objectives]The research aimed to determine the contents of moisture,ash and extract of wild Paeonia veitchii Lynch produced in Sichuan,so as to provide the basis for evaluating quality of wild P.veitchii Lynch from Sichuan.[Methods]Moisture,ash and extract contents of wild P.veitchii Lynch were respectively determined according to the fourth part of the Chinese Pharmacopoeia of 2015 version,and correlation analysis and TOPSIS analysis were used for data processing.[Results]12 batches of samples all corresponded with the provision that moisture of P.veitchii Lynch should not exceed 14.0%in the Standard of Traditional Chinese Medicine in Sichuan Province of 2010 version;11 batches of samples all corresponded with the provisions that total ash and acid insoluble ash of P.veitchii Lynch should not exceed 7.0%and 1.0%in the Standard of Traditional Chinese Medicine in Sichuan Province of 2010 version;average content of alcohol-soluble extract by hot dipping from 12 batches of samples was 42.29%,which was not less than 30.0%.In P.veitchii Lynch,moisture and acid insoluble ash showed positive correlation with altitude,while total ash and extract content were negatively correlated with altitude.Taking moisture,ash and extract as evaluation indexes,No.9 P.veitchii Lynch sample was the best.[Conclusions]Moisture and ash of P.veitchii Lynch corresponded with the provisions of the Chinese Pharmacopoeia of 2015 version and the Standard of Traditional Chinese Medicine in Sichuan Province of 2010 version,while extract content was higher than provision of the standard.The research could provide reference basis for rational utilization and quality evaluation of P.veitchii Lynch resources. 展开更多
关键词 PAEONIA veitchii LYNCH MOISTURE ash Extract content determination
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Quality Evaluation of Leontopodium franchetii Beauv. from Different Localities Based on Moisture,Ash and Extract Contents and Thin-layer Chromatography
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作者 Pei QUN Yatao HAN +3 位作者 Fang XIAO Zhe LIU Yongxia KE Yuan LIU 《Medicinal Plant》 CAS 2018年第4期56-58,共3页
[Objectives] The aim was to determine the moisture,ash and extract contents in Leontopodium franchetii Beauv. from different localities. [Methods] The contents of moisture,total ash,acid-insoluble ash and extract in L... [Objectives] The aim was to determine the moisture,ash and extract contents in Leontopodium franchetii Beauv. from different localities. [Methods] The contents of moisture,total ash,acid-insoluble ash and extract in L. franchetii from different localities were determined according to the methods described in Chinese Pharmacopoeia( 2015 Edition). [Results] In the 10 samples,the contents of moisture were all less than or equal to 15. 0%; the contents of total ash were all below 12. 0%; and the contents of acid-insoluble ash were all less than 3. 0%. The contents of water-soluble extract( by cold-soaked extraction method) in the samples were all below 12. 0% except those from Hongyuan Prairie of Sichuan Province and Xinglong Mountain in Lanzhou City,Gansu Province. [Conclusions]The contents of the four indicators measured in this experiment varied by small margins,indicating that the quality was relatively stable. This study provides theoretical data for the revision of the quality standards for L. franchetii. 展开更多
关键词 Leontopodium franchetii Beauv. MOISTURE ash Extract content Thin-layer chromatography Quality evaluation
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BOND PERFORMANCE EXPERIMENT FOR FLY ASH CONCRETE AND STEEL BAR
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作者 王倩 吴瑾 《Transactions of Nanjing University of Aeronautics and Astronautics》 EI 2012年第3期302-306,共5页
The impact of fly ash content on bond performance of steel bars and their surrounding concrete is studied by means of sticking strain gauges on steel bars. The average bond stress-slip curves, the steel strain-anchor ... The impact of fly ash content on bond performance of steel bars and their surrounding concrete is studied by means of sticking strain gauges on steel bars. The average bond stress-slip curves, the steel strain-anchor location curves, and the bond stress-anchor position curves of the pullout specimens with various fly ash contents are obtained. Results indicate that the bond performance of concrete and steel bars can be improved and the distribution of steel strain along the anchorage length tends to be more uniform by adding fly ash in concrete specimens, and both ultimate bond stress and ultimate slip deformation increase the most when 20% of specimens′ content is fly ash. 展开更多
关键词 fly ash concrete bond performance fly ash content bond stress distribution
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煤尘爆炸性与煤工业分析成分关系影响研究
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作者 胡夫 杨亚会 +1 位作者 钟敏 费宇 《煤炭技术》 CAS 2025年第1期156-159,共4页
采用大管状煤尘爆炸仪考查了不同工业分析指标与煤尘爆炸火焰长度的关系,实验结果表明,挥发分是影响煤尘爆炸性的主要因素,总体上呈现出挥发分越大,灰分越小,煤尘爆炸火焰长度越大的趋势。实验结果为通过煤的工业分析数据初步判断煤尘... 采用大管状煤尘爆炸仪考查了不同工业分析指标与煤尘爆炸火焰长度的关系,实验结果表明,挥发分是影响煤尘爆炸性的主要因素,总体上呈现出挥发分越大,灰分越小,煤尘爆炸火焰长度越大的趋势。实验结果为通过煤的工业分析数据初步判断煤尘的爆炸性提供了基础依据。 展开更多
关键词 煤尘 爆炸性 工业分析 挥发分 灰分
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不同橡胶粉灰分分析与改性沥青效果研究
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作者 王威 段丹军 +2 位作者 张波 高学凯 畅润田 《重庆交通大学学报(自然科学版)》 北大核心 2025年第2期75-81,共7页
废旧轮胎橡胶制品以及由其制备的橡胶粉类型众多,然而缺乏对不同类型废旧轮胎橡胶粉品质以及对沥青改性效果的系统研究。此外目前针对橡胶沥青中橡胶粉掺量的计量更是缺乏行之有效的检测方法。针对上述问题,首先,对尼龙胎、子午胎和轿车... 废旧轮胎橡胶制品以及由其制备的橡胶粉类型众多,然而缺乏对不同类型废旧轮胎橡胶粉品质以及对沥青改性效果的系统研究。此外目前针对橡胶沥青中橡胶粉掺量的计量更是缺乏行之有效的检测方法。针对上述问题,首先,对尼龙胎、子午胎和轿车胎3种橡胶粉灰分含量进行检测,探讨不同取样质量对灰分含量结果的影响;然后,借助能量色散型X射线荧光光谱分析仪(EDXRF)和X射线衍射仪(XRD)分别对3种橡胶粉灰分进行组成分析;最后,对比了20%、30%掺量的3种橡胶粉对沥青的性能提升效果。研究结果显示:取样质量对灰分含量结果检测影响很大,总体上灰分含量会随取样质量的增加而增大,且4种取样质量下,尼龙胎橡胶粉灰分含量均最小;3种橡胶粉灰分成分的共有且主要构成元素有4种,共有物质有6种,综合看来3种橡胶粉灰分的物质组成大体相似,但物质含量存在较大差异;对3种橡胶粉而言,掺量的增加均使得针入度下降,软化点、延度、黏度和弹性恢复升高,20%、30%掺量下尼龙胎橡胶粉对沥青综合性能提升效果最好。针对橡胶粉高温灰化条件下有灰分残留而沥青无残留的特点,提出可将橡胶粉中的灰分作为标记物,从而实现橡胶沥青中橡胶粉掺量的计量与检测。 展开更多
关键词 道路工程 橡胶粉 橡胶沥青 灰分 检测方法
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提高超重力油浆脱固工艺液体收率的方案研究
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作者 贺安新 赵福利 +2 位作者 闵正红 侯俊毅 古亚坤 《石油炼制与化工》 北大核心 2025年第2期59-64,共6页
液体收率是油浆脱固装置的重要指标,直接关系到经济效益和高灰分组分后处理的难度。超重力分离机采用定期排渣的方式将高灰分的渣浆排出,以保证装置稳定运行。为提高油浆脱固过程的液体收率,通过研究产品油浆灰分变化考察了排渣周期、... 液体收率是油浆脱固装置的重要指标,直接关系到经济效益和高灰分组分后处理的难度。超重力分离机采用定期排渣的方式将高灰分的渣浆排出,以保证装置稳定运行。为提高油浆脱固过程的液体收率,通过研究产品油浆灰分变化考察了排渣周期、进料流量和油相阻垢剂对排渣量的影响。试验结果表明:超重力分离机排渣周期越长,液体收率越高,但每处理0.4 t油浆必须进行一次排渣,否则将影响装置稳定性;通过加入油相阻垢剂,可有效减轻渣浆在设备内黏附,从而有助于渣浆排出;在油相阻垢剂加剂量(w)为100μg g的情况下,排渣周期可延长66.7%,液体收率提高到96.07%,具有较好的经济效益,且不会影响油浆后续利用。 展开更多
关键词 超重力分离机 油浆脱固 液体收率 灰分 渣浆 阻垢剂
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高砷次氧化锌灰低酸浸出液选择性硫化除砷技术研究
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作者 雷世麒 揭晓武 +1 位作者 张永禄 张坤坤 《有色金属(冶炼部分)》 CAS 北大核心 2025年第1期43-49,共7页
针对高砷次氧化锌灰多有价金属的高效回收,以及砷在锌冶炼系统的合理开路难题,以高砷次氧化锌灰三段逆流浸出得到的低酸浸出液为原液,研究了低酸液初始酸量、硫化剂量、反应时间、温度等因素对砷脱除效果及铟夹杂损失行为的影响。结果表... 针对高砷次氧化锌灰多有价金属的高效回收,以及砷在锌冶炼系统的合理开路难题,以高砷次氧化锌灰三段逆流浸出得到的低酸浸出液为原液,研究了低酸液初始酸量、硫化剂量、反应时间、温度等因素对砷脱除效果及铟夹杂损失行为的影响。结果表明,低酸液选择性硫化除砷效果显著,在初始酸量40 g/L、硫化钠用量为理论量的1.25倍、反应时间2 h、温度70℃等优化工艺条件下,沉砷后液砷含量<1 g/L,砷脱除率达88.09%,铟损失率仅为8.15%,砷沉淀率/铟损失率比值达11,硫化砷渣中As含量达32.77%,为锌冶炼砷的合理开路提供新的思路。 展开更多
关键词 次氧化锌灰 高砷 硫化沉砷 砷铟分离
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根据精煤产率最大化原则(等λ原则)测算精煤指标控制区间的研究
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作者 高玉辉 李明远 +1 位作者 李作全 崔振 《煤炭加工与综合利用》 2025年第1期29-32,共4页
基于产率最大化原则,通过对秦华煤矿选煤厂进行生产数据整理、分析及计算,在基元灰分条件下查询各分选环节可选性曲线,确定各环节精煤灰分及产率,以确定三个分选环节最佳灰分控制区间。研究结果表明:各分选环节精煤灰分在指标要求上限... 基于产率最大化原则,通过对秦华煤矿选煤厂进行生产数据整理、分析及计算,在基元灰分条件下查询各分选环节可选性曲线,确定各环节精煤灰分及产率,以确定三个分选环节最佳灰分控制区间。研究结果表明:各分选环节精煤灰分在指标要求上限值范围内(±1%)波动,各分选环节累计精煤灰分为指标要求灰分时,精煤产率累计值最大。 展开更多
关键词 精煤产率最大化 等λ原则 基元灰分 可选性曲线 最佳灰分
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煤炭中灰分及挥发分对发热量的影响研究
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作者 赵积坤 《化工管理》 2025年第1期63-65,共3页
煤炭发热量是指煤炭燃烧时发出的能量,煤炭的发热量是评价煤质的重要指标,反映了单位质量煤炭完全燃烧后所放出的全部热量。煤炭的发热量不仅用于鉴定煤质、计算热平衡和耗煤量,还是改进燃煤方法、提高热能利用效率的依据。文章通过多... 煤炭发热量是指煤炭燃烧时发出的能量,煤炭的发热量是评价煤质的重要指标,反映了单位质量煤炭完全燃烧后所放出的全部热量。煤炭的发热量不仅用于鉴定煤质、计算热平衡和耗煤量,还是改进燃煤方法、提高热能利用效率的依据。文章通过多年来多批次煤炭的测定、分析、总结得出煤中灰分、挥发分对发热量的影响。 展开更多
关键词 发热量 灰分 挥发分 影响因素
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煤质分析在选煤工艺选择中的应用
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作者 李佳念 《能源与节能》 2025年第1期330-332,336,共4页
为优化选煤工艺并提高煤炭资源利用效率,针对不同煤质参数(如热值、灰分、水分、含硫量)工艺选择分析,以煤炭行业选煤技术干选、水洗、重介质分离、浮游选煤法、电力选煤法和脱泥筛选为例,分析了各种煤质参数对选煤工艺的影响。结果表明... 为优化选煤工艺并提高煤炭资源利用效率,针对不同煤质参数(如热值、灰分、水分、含硫量)工艺选择分析,以煤炭行业选煤技术干选、水洗、重介质分离、浮游选煤法、电力选煤法和脱泥筛选为例,分析了各种煤质参数对选煤工艺的影响。结果表明,通过精确煤质分析与匹配适宜工艺,可有效提升煤炭质量和燃烧效率,降低环境污染和处理成本。例如低灰分煤炭适宜采用物理选煤处理以保留热值,高水分煤炭则需先进行干燥、脱水处理。对含硫量不同的煤炭,根据具体含量选择从简单物理处理到复杂化学处理策略。研究结果可为煤炭行业提供最优选煤工艺依据。 展开更多
关键词 煤质分析 选煤工艺 低灰分煤炭 含硫量
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干灰化-碳酸钠碱熔-电感耦合等离子体发射光谱法测定植物样品中硅含量
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作者 许熔熔 阮泽斌 +1 位作者 胡铁军 周飞 《浙江农业科学》 2025年第1期155-159,共5页
该研究建立了一种通过干灰化-碳酸钠碱熔-电感耦合等离子体发射光谱法(ICP-OES)测定植物样品中硅(Si)含量的方法。即根据不同种类样品中的灰分含量,将适量样品经马弗炉灼在600℃条件下灰化,然后加入碳酸钠在950℃熔融,使用稀盐酸溶液提... 该研究建立了一种通过干灰化-碳酸钠碱熔-电感耦合等离子体发射光谱法(ICP-OES)测定植物样品中硅(Si)含量的方法。即根据不同种类样品中的灰分含量,将适量样品经马弗炉灼在600℃条件下灰化,然后加入碳酸钠在950℃熔融,使用稀盐酸溶液提取熔块后,用ICP-OES测得Si含量。结果表明,该方法在最佳试验条件下,检出限为6 mg·kg^(-1),测定下限为24 mg·kg^(-1),精密度和准确度符合相关规范要求。将所建方法应用于实际植物样品中的Si含量测试,其测定结果与标准物质的相对误差在-16.4%~10.5%,满足《生态地球化学评价生物样品技术要求》(DD2005-03)中对分析准确度的要求,即分析平均值与标准物质推荐值的相对误差RE≤30%。 展开更多
关键词 干灰化 碱熔 植物样品 硅含量
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矿物掺合料对泡沫混凝土性能的影响
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作者 刘柏君 张国防 +2 位作者 郑薇 应灵慧 陆小培 《建筑材料学报》 北大核心 2025年第3期252-260,共9页
开展了粉煤灰(FA)、矿渣微粉(GBFS)、提钛尾渣(TS)等3种矿物掺合料对泡沫混凝土性能影响的研究.结果表明:3种掺合料均能在一定程度上提高泡沫混凝土的体积密度,其中TS的影响尤为明显;GBFS会降低泡沫混凝土的流动度,但TS和低掺量FA能提... 开展了粉煤灰(FA)、矿渣微粉(GBFS)、提钛尾渣(TS)等3种矿物掺合料对泡沫混凝土性能影响的研究.结果表明:3种掺合料均能在一定程度上提高泡沫混凝土的体积密度,其中TS的影响尤为明显;GBFS会降低泡沫混凝土的流动度,但TS和低掺量FA能提高其流动度;3种矿物掺合料在低掺量时均能提高泡沫混凝土的体积吸水率和毛细吸水率,但在较高掺量时,又降低了其体积吸水率和毛细吸水率,其中TS和GBFS的降低作用尤为明显;3种矿物掺合料在高掺量时均能明显提高泡沫混凝土的抗压强度,其中TS的提升效果最好;FA和GBFS提高了泡沫混凝土的28 d干燥收缩率,TS则显著降低其28 d干燥收缩率;综合而言,FA和GBFS最佳掺量范围均为10%~15%,TS为5%~15%. 展开更多
关键词 泡沫混凝土 粉煤灰 矿渣微粉 提钛尾渣 性能 最佳掺量
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