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胶体金/DNA体系法快速测定不同水质中银离子 被引量:2
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作者 程晓宏 谢超 史玉坤 《交通医学》 2013年第1期27-28,31,共3页
目的:建立简单、快速检测银离子的新方法。方法:建立简单、快速检测银离子胶体金/DNA体系方法,利用分光光度计扫描加入银离子前、后胶体金/DNA体系光谱,通过比较加入银离子前、后A660/A530大小来快速定量银离子。加入银离子后,体系A66... 目的:建立简单、快速检测银离子的新方法。方法:建立简单、快速检测银离子胶体金/DNA体系方法,利用分光光度计扫描加入银离子前、后胶体金/DNA体系光谱,通过比较加入银离子前、后A660/A530大小来快速定量银离子。加入银离子后,体系A660/A530变化较其他离子大,颜色由红色变成蓝色。结果:该方法的线性范围为0.1~2.0μg/mL,检出限为0.05μg/mL,线性相关系数r=0.999。结论:该法应用于不同水质中银的测定,简单、快速、准确,结果满意。 展开更多
关键词 胶体金 DNA 胞嘧啶C碱基 分光光度计扫描法 胶体金 DNA体系检测
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Photocatalytic activity of bauxite-tailings supported nano-TiO_2
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作者 卢清华 胡岳华 王梦 《Journal of Central South University》 SCIE EI CAS 2010年第4期755-759,共5页
TiO2/bauxite-tailings (TiO2/BTs) composites were prepared via a chemical liquid deposition method and characterized by X-ray diffractometry (XRD), scanning electronic microscopy (SEM) and N2 adsorption analysis.... TiO2/bauxite-tailings (TiO2/BTs) composites were prepared via a chemical liquid deposition method and characterized by X-ray diffractometry (XRD), scanning electronic microscopy (SEM) and N2 adsorption analysis. The photocatalytic performance of TiO2/BTs composites was evaluated with UV-Vis spectrophotometer following the changes of phenol concentration under different illumination time. Effects of the calcination temperature, the pH and the cycles on the photocatalytic activity of TiO2/BTs composites were investigated. The composites calcined at 500 and 600 ℃ exhibit the best photocatalytic performance, and the phenol degradation ratios reacting for 40 and 160 rain reach 35% and 78% respectively under the same conditions, higher than those of 29% and 76% of the Degussa P25(TiO2). The ability of TiO2/BTs500 (BTs500 represents bauxite-tailings calcined at 500 ℃) composites to degrade phenol increases with decreasing pH. 展开更多
关键词 TIO2 bauxite-tailings PHENOL photocatalytic activity
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